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Published in:

Volume 7 Issue 3
March-2020
eISSN: 2349-5162

Unique Identifier

JETIRDN06045

Page Number

196-198

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Title

SYNTHESIS, SPECTRAL AND XRD STUDIES OF SCHIFF-BASE LIGAND AND A SERIES OF 1. 10-PHENANTHOLINE TRANSITION METAL COMPLEXES

ISSN

2349-5162

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"SYNTHESIS, SPECTRAL AND XRD STUDIES OF SCHIFF-BASE LIGAND AND A SERIES OF 1. 10-PHENANTHOLINE TRANSITION METAL COMPLEXES ", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.7, Issue 3, page no.196-198, March-2020, Available :http://www.jetir.org/papers/JETIRDN06045.pdf

Abstract

1,10-phenanthroline transition metal complexes of the type [M(phen)2(L)](OAc)2.(nH2O) containing Schiff base ligands derived from 2-chloro ethyl amine and 2-hydroxy-3,5-diiodo benzaldehyde were synthesized and characterized by elemental analysis, Powder XRD, UV–vis, IR, 1H NMR, spectral methods. Elemental analysis data revealed that the complexes have a 1:2:1 molar ratio among the metal and ligands. The IR and 1H NMR, spectral data confirmed that the ligands coordinate with the metal ions in a bidentate fashion through azomethine nitrogen and phenolic oxygen to form complexes. Powder XRD shows the sharp crystalline peaks indicating the crystalline state of the complexes.

Key Words

1,10 phenanthroline transition metal complexes, 2-chloro ethyl amine,

Cite This Article

"SYNTHESIS, SPECTRAL AND XRD STUDIES OF SCHIFF-BASE LIGAND AND A SERIES OF 1. 10-PHENANTHOLINE TRANSITION METAL COMPLEXES ", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.7, Issue 3, page no. pp196-198, March-2020, Available at : http://www.jetir.org/papers/JETIRDN06045.pdf

Publication Details

Published Paper ID: JETIRDN06045
Registration ID: 229495
Published In: Volume 7 | Issue 3 | Year March-2020
DOI (Digital Object Identifier):
Page No: 196-198
ISSN Number: 2349-5162

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Cite This Article

"SYNTHESIS, SPECTRAL AND XRD STUDIES OF SCHIFF-BASE LIGAND AND A SERIES OF 1. 10-PHENANTHOLINE TRANSITION METAL COMPLEXES ", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.7, Issue 3, page no. pp196-198, March-2020, Available at : http://www.jetir.org/papers/JETIRDN06045.pdf




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