• Khaled W. Shaikh
• Chandrakant V. Magar

1,10-phenanthroline transition metal complexes of the type [M(phen)2(L)](OAc)2.(nH2O) containing Schiff base ligands derived from 2-chloro ethyl amine and 2-hydroxy-3,5-diiodo benzaldehyde were synthesized and characterized by elemental analysis, Powder XRD, UV–vis, IR, 1H NMR, spectral methods. Elemental analysis data revealed that the complexes have a 1:2:1 molar ratio among the metal and ligands. The IR and 1H NMR, spectral data confirmed that the ligands coordinate with the metal ions in a bidentate fashion through azomethine nitrogen and phenolic oxygen to form complexes. Powder XRD shows the sharp crystalline peaks indicating the crystalline state of the complexes.

1,10 phenanthroline transition metal complexes, 2-chloro ethyl amine,

"SYNTHESIS, SPECTRAL AND XRD STUDIES OF SCHIFF-BASE LIGAND AND A SERIES OF 1. 10-PHENANTHOLINE TRANSITION METAL COMPLEXES ", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.7, Issue 3, page no.196-198, March-2020, Available :http://www.jetir.org/papers/JETIRDN06045.pdf

"SYNTHESIS, SPECTRAL AND XRD STUDIES OF SCHIFF-BASE LIGAND AND A SERIES OF 1. 10-PHENANTHOLINE TRANSITION METAL COMPLEXES ", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.7, Issue 3, page no. pp196-198, March-2020, Available at : http://www.jetir.org/papers/JETIRDN06045.pdf