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Published in:

Volume 7 Issue 3
March-2020
eISSN: 2349-5162

Unique Identifier

JETIRDN06055

Page Number

238-241

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Title

Solvent free and High yielding Synthesis of new dimethyl 1-(2-chloroquinolin-3-yl)-2,2-dicyanoethylphosphonate from 2-chloroquinoline-3-carbaldehyde

ISSN

2349-5162

Cite This Article

"Solvent free and High yielding Synthesis of new dimethyl 1-(2-chloroquinolin-3-yl)-2,2-dicyanoethylphosphonate from 2-chloroquinoline-3-carbaldehyde", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.7, Issue 3, page no.238-241, March-2020, Available :http://www.jetir.org/papers/JETIRDN06055.pdf

Abstract

A simple solvent free and high yielding method was developed for the synthesis of new derivatives of dimethyl 1-(2-chloroquinolin-3-yl)-2,2-dicyanoethylphosphonate from 2-((2-chloroquinolin-3-yl)methylene)malononitrile, obtained from 2-chloroquinolin-3-carbaldehydes by using dimethylphosphite in the presence of DBU as catalyst at room temperature. All the synthesized compounds were characterized by IR, 1HNMR, Mass spectroscopy.

Key Words

2-chloroquinoline-3-carbaldehyde, Knoevenagel condensation, Michael addition, dimethylphosphite, DBU.

Cite This Article

"Solvent free and High yielding Synthesis of new dimethyl 1-(2-chloroquinolin-3-yl)-2,2-dicyanoethylphosphonate from 2-chloroquinoline-3-carbaldehyde", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.7, Issue 3, page no. pp238-241, March-2020, Available at : http://www.jetir.org/papers/JETIRDN06055.pdf

Publication Details

Published Paper ID: JETIRDN06055
Registration ID: 229484
Published In: Volume 7 | Issue 3 | Year March-2020
DOI (Digital Object Identifier):
Page No: 238-241
ISSN Number: 2349-5162

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Cite This Article

"Solvent free and High yielding Synthesis of new dimethyl 1-(2-chloroquinolin-3-yl)-2,2-dicyanoethylphosphonate from 2-chloroquinoline-3-carbaldehyde", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.7, Issue 3, page no. pp238-241, March-2020, Available at : http://www.jetir.org/papers/JETIRDN06055.pdf




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