UGC Approved Journal no 63975(19)

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Published in:

Volume 4 Issue 10
October-2017
eISSN: 2349-5162

UGC and ISSN approved 7.95 impact factor UGC Approved Journal no 63975

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Published Paper ID:
JETIR1710122


Registration ID:
304203

Page Number

790-792

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Title

SYNTHESIS AND CHARACTERIZATION OF A TRINUCLEAR Ni(II) COMPLEXES WITH TRICOMPARTMENTAL MACROCYCLIC LIGAND

Abstract

Kinetic template reaction between nickel bromide, glyoxal and hydrazine develops blue crystals of [Ni(GDFI)2Br2] on one hand and green crystals of 13, 14- exocyclicdioxo-1, 5, 8. 12-tetraaza-2, 3 : 10,1 I-dibenzocyclotetradeca-2. 4, 8, 10-tetraenato [2-] nickel (II) by kinetic template condensation of nickel acetate. salicylaldehyde and 1:2- diaminoethane on the other. Finally the blue and green crystals are allowed to undergo self assembly process in the molar ratio 1:2 in DMF medium under nitrogen at 100°C to produce orange red crystals of a trinuclear nickel (II) clathrochelate. The compound has been characterized with elemental analysis. conductivity and magnetic susceptibility measurements, infrared and visible spectral studies. The nickel(11) ions are found to be in different stereochcmical environments.

Key Words

Clathrochelate, spectral studies, tricompartmental ligand.

Cite This Article

"SYNTHESIS AND CHARACTERIZATION OF A TRINUCLEAR Ni(II) COMPLEXES WITH TRICOMPARTMENTAL MACROCYCLIC LIGAND", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.4, Issue 10, page no.790-792, October-2017, Available :http://www.jetir.org/papers/JETIR1710122.pdf

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2349-5162 | Impact Factor 7.95 Calculate by Google Scholar

An International Scholarly Open Access Journal, Peer-Reviewed, Refereed Journal Impact Factor 7.95 Calculate by Google Scholar and Semantic Scholar | AI-Powered Research Tool, Multidisciplinary, Monthly, Multilanguage Journal Indexing in All Major Database & Metadata, Citation Generator

Cite This Article

"SYNTHESIS AND CHARACTERIZATION OF A TRINUCLEAR Ni(II) COMPLEXES WITH TRICOMPARTMENTAL MACROCYCLIC LIGAND", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.4, Issue 10, page no. pp790-792, October-2017, Available at : http://www.jetir.org/papers/JETIR1710122.pdf

Publication Details

Published Paper ID: JETIR1710122
Registration ID: 304203
Published In: Volume 4 | Issue 10 | Year October-2017
DOI (Digital Object Identifier):
Page No: 790-792
Country: Muzaffarpur, Bihar, India .
Area: Chemistry
ISSN Number: 2349-5162
Publisher: IJ Publication


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