• T. R. Tatte
• S. V. Agnihotri

Magnesium ferrite (MgFe2O4) nanoparticles were synthesized using a sol-gel synthesis method using citric acid as anionic surfactant and synthesized particles were calcinated at 700°C. X-ray diffraction data confirm the formation of single-phase cubic structure and the average grain sizes were evaluated. The XRD result revealed the production of a sharp single cubic spinel structure of prepared sample without any impurity peak with the crystallite size of about 33.29 nm. The high and low frequency absorption bands of MgFe2O4 were investigated using FT-IR analysis. The microstructural features were examined by scanning electron microscopy (SEM) and transmission electron microscopy (TEM) and compositional analysis carried out by energy dispersive X-ray analysis (EDS).

Nano ferrite, XRD, FT-IR, SEM, EDX, TEM.

"Synthesis and Characterization of Nanocrystalline Spinel Magnesium Ferrite Prepared by Sol-Gel Method", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.9, Issue 5, page no.b102-b107, May-2022, Available :http://www.jetir.org/papers/JETIR2205116.pdf

"Synthesis and Characterization of Nanocrystalline Spinel Magnesium Ferrite Prepared by Sol-Gel Method", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.9, Issue 5, page no. ppb102-b107, May-2022, Available at : http://www.jetir.org/papers/JETIR2205116.pdf