• Nitin Upadhyay
• Dr. B. D. Shrivastava
• Dr. Ashutosh Mishra

As part of a continuing search for the synthesis of new antimicrobial agents, some macrocyclic tetradentate nitrogen donor (N4) ligand based transition metal complexes of the type [ML1-5] where M= Cu(II), L1-L5 were of our interest. All new metal complexes of transition metal ion containing Cu (II) and ligands [ L1 –L5] were synthesized. The ligands were prepared by chemical root procedure which included the reaction of pyridin-2-carboxaldehyde with alkyl amines. The XRD data has been obtained by PDXL software. From the experimental measurements, various parameters such as lattice parameter and particle size have been estimated. Particle size is found to be in the range of nanometres. The XRD analysis of the complexes revealed the crystalline nature.

XRD ,Synthesis of copper metal complexes

"SYNTHESIS AND XRD CHARACTERIZATION OF COPPER (II) CONTAINING METAL COMPLEXES", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.9, Issue 9, page no.a641-a643, September-2022, Available :http://www.jetir.org/papers/JETIR2209067.pdf

"SYNTHESIS AND XRD CHARACTERIZATION OF COPPER (II) CONTAINING METAL COMPLEXES", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.9, Issue 9, page no. ppa641-a643, September-2022, Available at : http://www.jetir.org/papers/JETIR2209067.pdf