• Mala Mangwani
• B D Shrivastava
• A Mishra

In this paper we have discussed preparation of iron complex with ligand (1E,3E,6E,9E)-4,6,10,12-tetramethyl-5,11-bis(E)-p-tolyldiazenyl)-1,3,7,0-tetraazacyclodeca-3,6,9,12-tetraenebase and its x ray absorption studies. EXAFS is a spectroscopic method used to find the distances of metal its nearest neighboring atoms . XRD characterization has been done in order to estimate the crystallite size. In present paper nearest neighboring distances have been calculated using various graphical methods like Levy’s, Lytle’s and LSS method. The distance is also calculated theoretically using Fourier Transform method. The values obtained from graphical methods are found to be very close with the distance estimated using Fourier transform method .With the help of XANES spectra the position of principal maxima and k edge is found.

XRD, X-ray absorption spectroscopic study and synthesis of iron complex

"XRD, X-ray absorption spectroscopic study and synthesis of iron complex ", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.10, Issue 9, page no.d113-d116, September-2023, Available :http://www.jetir.org/papers/JETIR2309313.pdf

"XRD, X-ray absorption spectroscopic study and synthesis of iron complex ", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.10, Issue 9, page no. ppd113-d116, September-2023, Available at : http://www.jetir.org/papers/JETIR2309313.pdf