UGC Approved Journal no 63975(19)

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Published in:

Volume 6 Issue 5
May-2019
eISSN: 2349-5162

UGC and ISSN approved 7.95 impact factor UGC Approved Journal no 63975

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Published Paper ID:
JETIRCU06025


Registration ID:
218074

Page Number

112-121

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Title

Synthesis of Amyl acetate using a Silica supported Heteropoly acid- A Kinetic Study

Abstract

There is an increase in the inclination of chemical industries towards new processes that should meet the requirements such as the generation of nearly zero waste chemicals, less energy and sufficient use of product chemicals in various applications. Esterification is one of the most widely employed reactions in the organic process industry. Most esterification reactions employ liquid acids as catalysts that cannot be recovered and also tend to corrode the reactors. This necessitates the use of heterogeneous eco-friendly catalysts. The present work focuses on the synthesis of isoamyl acetate using silica supported heteropoly acid. The catalyst was prepared by precipitation method. The performance of the catalyst was studied for the synthesis of isoamyl acetate at various reaction conditions such as mole ratio of reactants, temperature and catalyst loading. It was observed maximum acetic acid conversion of 90% was attained at 100oC, 1:3 and 3w/w% catalyst loading. Further, the kinetic studies were done and the activation energy was determined by the Arhennius equation as 33.76 kJ/mol.

Key Words

Esterification, Heteropoly acid, Kinetics, Activation energy

Cite This Article

"Synthesis of Amyl acetate using a Silica supported Heteropoly acid- A Kinetic Study", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.6, Issue 5, page no.112-121, May 2019, Available :http://www.jetir.org/papers/JETIRCU06025.pdf

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2349-5162 | Impact Factor 7.95 Calculate by Google Scholar

An International Scholarly Open Access Journal, Peer-Reviewed, Refereed Journal Impact Factor 7.95 Calculate by Google Scholar and Semantic Scholar | AI-Powered Research Tool, Multidisciplinary, Monthly, Multilanguage Journal Indexing in All Major Database & Metadata, Citation Generator

Cite This Article

"Synthesis of Amyl acetate using a Silica supported Heteropoly acid- A Kinetic Study", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.6, Issue 5, page no. pp112-121, May 2019, Available at : http://www.jetir.org/papers/JETIRCU06025.pdf

Publication Details

Published Paper ID: JETIRCU06025
Registration ID: 218074
Published In: Volume 6 | Issue 5 | Year May-2019
DOI (Digital Object Identifier):
Page No: 112-121
Country: Chennai, Tamil Nadu, India .
Area: Engineering
ISSN Number: 2349-5162
Publisher: IJ Publication


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